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GXZ HIGH EFFICIENCY ROTATION THIN FILM EVAPORATOR 

1. Introduction
GXZ Series Rotation Thin Film Evaporator manufactured by Wuxi Lima Chemical Machinery Co.,Ltd. ( former Wuxi Chemical Machinery Factory ) is a new type of high efficiency evaporator which uses rotating scratch blade to force forming film and create falling film evaporation under vacuum condition. It has big heat transferring coefficient, high evaporation strength, short overflow time, flexible operation property etc. advantages, suitable for heat sensitive materials, high viscose materials, and easy crystallization, containing powder materials evaporation, concentration, degassing, de-solving, distillation purification. Due to these advantages, it is widely used in petrochemical, chemical, pharmaceutics, pesticide, daily chemical, food processing and fine chemical industries.
We have manufactured this type equipment for more than 10 years and gained plenty of fabrication and application experiences. According to market demanding, combined with customer¡¯s production requirements, and to meet clients¡¯ process requirement, we select optimized equipment structure to assure reliable and top fabrication quality. By improving fabrication equipment, testing method and production design, we reached remarkable achievements. We are at domestic leading position in technical level and products quality. This product has passed Jiangsu Provincial Science and Technological Achievements Appraisal ( No.03,1994) in Jan.,1994 and received ¡°National Grade New Product Honor¡± in 1995 and applied Patent from China Patent Bureau in 1999 ( Patent No. ZL 99 2 28920.3).
2. Structure
GXZ Series Thin Film Evaporator Main Structure see Figure 1, The detailed components see the following description:
a. Motor, Speed Reducer
It is the device driven by rotor rotation. The rotor rotation speed is decided by scraper shape, materials viscosity and the inner diameter of evaporation column. To select proper scraper linear velocity is one of the important parameters to assure evaporator stable and reliable operation and get satisfaction of evaporation result.
b. Separation Column
The materials enter the evaporator in the inlet located at the bottom of separation column by tangent direction and uniformly distributed on the inner wall of evaporator column by distributor in the column. The second time vapor evaporated from evaporator column goes up to separation column, the liquid drops and bubbles which possibly entrained in the vapor will be separated out by gas/liquid separator, the second time vapor goes out from evaporator through top location exit.
The optimized design of separation column based on the evaporator inner resistance calculation is the key element of avoiding materials ¡°short cut¡±. (¡°Short Cut¡± means that the entered materials fail to complete evaporation process but escape from the second time vapor exit of evaporator).
c. Distributor
The distributor is located on the rotor. The rational design makes materials enter evaporator in tangent direction ( see figure 1 indication ) and continuously , uniformly to be distributed on evaporation surface in film form.

d. Gas/Liquid Separator
The rotating scraper type gas/liquid separator is installed on the up location of the separation column. The function is to capture entrained liquid drops and bubbles in the second time vapor and make them to drop back to the evaporation surface.
e. Evaporation Column
Also called Heating Column. It is the heat exchanging evaporation surface between materials film, which is formed to be forced by rotating scraper and heating medium in the jacket. The inner diameter and length of heating column are determined by evaporation surface and proper length/diameter ratio.
The heating column inner wall is machined and polished by special machinery and formed with both ends flange connection surface in one time, which assures the whole equipment roundness. After polishing ( if necessary mirror polishing), the inner wall of the column is smooth and brilliant, not easy to stick materials and scared, as a result, effectively assures equipment high heat transfer coefficient.

¢ÙThe jacket is used for column heating if the heating media is steam.
    ¢ÚThe half pipe shape jacket is used for column heating, if the heating media is heat oil or high pressure steam.
    f. Rotor
    The rotor installed in evaporator inside consists of rotating shaft and support. The rotor driven by motor and speed reducer brings scraper to make circular movement. The support is made stainless steel and machined in precise dimensions to assure the strength, dimension, and stability etc. properties.
    g. Scraper
    The scraper movement makes materials form thin film continuously on evaporator surface to reach the thin film evaporation results.

According to viscosity of the materials, the following three types scrapers can be selected:
    ¢ÙSlide Scraper (see figure 2)
    Sliding scraper is a basic and normal scraper. The scrapers are installed in the four guiding grooves on the rotor. Due to the rotation centrifugal force, the scrapers circular movement force materials to move towards column inner wall in radial direction and make the materials on evaporation surface in film turbulent form. Thus, greatly increase the heat transfer coefficient and effectively avoid materials overheat, drying wall and scarring etc. problems.

The scrapers use PTFE as packing materials, it is suitable at 150¡æ working temperature. If the evaporation temperature is above 150¡æ,carbon fiber materials will be used as packing. The scraper end surface is machined to form certain angular liquid guide groove.

¢ÚFixed Scraper see (figure 3)
    Fixed in rotor, the scraper is made of metal materials, The gap distance between rotating scraper and the inner wall of column is only 1-2mm. It requires high fabrication and installation precision. It is suitable for high viscose and easy bubbling materials evaporation and concentration, de-solving and extraction.
    ¢ÛHinge Scraper ( See Figure 4)

This kind of scraper is suitable for easy scaring materials on heating surface. The scraper usually is made of metal. It is fixed on the rotating frames by means of hinges. When the rotor starts rotation, because of centrifuge force, the scraper will be tightly pressed to the inner wall of evaporation column (and wall surface), sliding on the surface in certain angles to make materials into thin film and prevent from scaring on the surface. 
H. Bottom Head
    W shape bottom head with unique design, equipped with high temperature resistance, self-lubricating bearings makes materials easy discharging and bottom shaft convenient maintenance and repairing.
    3.Characteristics:
    Thin film evaporator has the following advantages, which the normal film evaporator has no way to compare with.
a. Extreme small pressure loss
    In rotation scraper thin film evaporator, the materials ¡°stream¡± and second vapor ¡° stream¡± are two independent ¡°through channel¡±: The materials fall down in thin film status ( force to form film ) against inner wall of evaporator column, while the second vapor evaporated from evaporation surface goes out almost without any resistance from the central space of column. Therefore, the pressure lost (or call pressure drop) is very small. So,
    b. The operation in the real vacuum status can be obtained.
    Because the second vapor resistance from surface to condensate is very small, the inner wall evaporation surface in the whole evaporation column can maintain relatively high vacuum degree (more than -750mmHg),almost equal to the vacuum degree in the exit of vacuum system. Due to maintain high vacuum degree, the boiling point of the treated material is effectively lowered.
    c. High heat transfer coefficient, high evaporation strength
    The materials boiling point decreasing greatly increases temperature difference with heat medium, the liquid film in turbulent status reduces the heat resistance, also, inhibits materials scarring on the wall surface, as a result, increase evaporation column wall sub-heat transfer coefficient. The total heat transfer coefficient of high efficient rotation thin film evaporator may reach 8000KJ/h¡¤©O¡¤¡æ which is very high evaporation strength.
    d. Low temperature evaporation
    Because relatively high vacuum degree is maintained in the evaporator column, the treated materials boiling point decreased greatly, it is especially suitable for the heat sensitive materials evaporation at low temperature.

 e. Short flow pass
    The flow time in the evaporator is very short. Less than 10 seconds. For normal use scraper, there is flow-guiding groove on the scraper end face, usually the slope angle is 45. To change the slope angle may change materials flow time. The material scrapped by scraper leaves evaporator sector in screw falling status. To shorter flow time will effectively prevent from products decomposing, polymerization and deterioration.
    f. Low quality steam can be used.
    Steam is commonly used heating media. Because the materials boiling point is decreased, as long as assuring the same ¦¤t condition, the heating media temperature can be decreased. To use low quality vapor is helpful for energy multiple use, especially suitable for the end evaporator of multiple-effect evaporation.
    g. Versatile Suitability, Easy Operation
    Unique structure design makes this equipment possibly treat high viscosity, particle containing, heat sensitive and easy crystallization materials which the normal evaporator is difficult to treat with.
    The rotation thin film evaporator has wide operation range, stable working status, and easy maintenance.
    4. Products Specification

Specification Definition for GXZ High Efficiency Rotation Thin Film Evaporator:
    GXZ High Efficiency Rotation Thin Film Evaporator Dimensions and partly Technical Parameters see Figure 6 and Table 1
    Figure 1: GXZ High Efficiency Rotation Thin Film Evaporator Dimensions and partly Technical Parameters see Figure 6 and Table 1

Evaporation
Surface
(m2)
Size
Equip.
Total
Height
A
Heating
Column
Height
B
Feeding
Materials
Separation
Column
C
Column
OD.
D
Support
Height
E
Motor
Speed
Reducer
F
Hole
Gap
of
Support
G
Dn
0.3 2290 750 550 273 1253 702 480 211
0.5 2440 900 550 273 1403 702 480 211
1 2820 1200 550 412 1781 702 605 313
2 4330 1830 755 462 2372 1433 843 400
4 5490 2630 844 712 3511 1565 1003 600
6 6275 2890 844 912 3817 1944 1236 800
8 6910 3658 844 916 4587 1909 1236 800
10 6960 3658 900 1112 4542 1918 1236 1000
12 7460 3658 1003 1316 4985 1998 1567 1200
15 8315 4590 1003 1316 4390 2040 1804 1200
18 9210 5494 1003 1316 5290 2040 1804 1200
20 9840 6121 1003 1316 5920 2040 1804 1200
Evaporation
Surface
(m2)
Equipment
Motor Power
(kW)
Pressure (Mpa) Total weight
(about)(Kg)
Jacket Inner Column
0.3 1.5 0.6 £¼-0.095 480
0.5 1.5 0.6 £¼-0.095 500
1 1.5 0.6 £¼-0.095 680
2 3.0 0.4 £¼-0.095 1100
4 5.5 0.4 £¼-0.095 1950
6 7.5 0.4 £¼-0.095 2980
8 7.5 0.4 £¼-0.095 3550
10 7.5 0.4 £¼-0.095 4880
12 11 0.4 £¼-0.095 6300
15 15 0.4 £¼-0.095 7850
18 15 0.4 £¼-0.095 8830
20 15 0.4 £¼-0.095 9350

¢ÙThere are possible change for the above dimensions in actual equipment, reference only. Take the drawings dimension as actual size after signed purchase order.
    ¢ÚD indicates jacket outer diameter; Dn indicates inner diameter of evaporation column in the table.
    ¢ÛJacket Pressure: Normally designed based on 0.4Mpa steam, also can be designed per customer requirement.
If heating oil is used, it can be designed per the requirement.
    ¢ÜThe vacuum degree in the inner evaporation column : Normally designed based on -0.09Mpa(-680mmHg), also can meet clients¡¯ requirement to reach -0.095Mpa(about -720mmHg)and -0.0986Mpa(about-750mmHg)£»
    ¢ÝMain Column ( Materials contacting parts) and jacket materials: Per clients¡¯ actual requirements, use SUS304¡¢316L¡¢316Ti¡¢.310Sor Ti and Ni. Materials£»
    ¢ÞEquipment Total Weight does not include materials weight.
    5. Application Industries and Operation Unit Sample
    High Efficiency Rotation Thin Film Evaporator has been widely used for Chinese and West Medicine, Agriculture Pesticide, Light Industry, Daily Chemical, Biological Chemical, Fine Chemical, Petrochemical etc. industries. Excellent results have been received. See Table (2), reference only.

Industry Typical
Materials
Industry Typical
Materials
Industry Typical
Materials
Pharmaceu-
tics
Vitamin VE¡¢V Inorganic TiCl3 Organic High
Concentration
Aldehyde
Chinese Herb MnO2 Fine
terephthalic
salts
Anti-bacteria
Agent
Caustic Soda Trihydroxymethyl
propane
Pharmaceutics
Solution
K2SO4 xanthate
aldehyde
Medical
Intermediate
KBr, NaBr Poly ether
polyol
Nitrile Amine Aluminum Sulfates Peach glue
Azoles Sodium Silicate Polyacrylamine
Light
Industry
and
Daily
Chemical
Natural
Colorant
KNO3 Tetra-amino-
aniline
Lactic Acid
L-Lactic Acid
Potassium
permanganate
Tri-methyl
Quinone
Lacithin Calcium sulfide Epoxy Resin
Essence Tungstic acid
Molybdic acid
Bis-phenol -A
Bee Honey Sodium
Hydrosulfite
Rongalite
Methy,
Ethyl Ester
Carbonates
Glyceryl Pesticide Furan phenol Hydroxyl
acetic acid
Animal Feed
Additives
Pyrethrin
Environment
Protection
Waste Water of
Sodium Sulfates
Starch
Glycogen
Ethyl ammonium
oxalate
Waste Water of
NaCl
Enzyme Methamidophos Waste Water of
NH4Cl
Alkyl
glyciside
Tetrahydrofuran Waste Water of
(NH4)2SO4
Alcohol Ether
Sulfates
Weed-killer  
Potassium
sorbate
   
Dextran
calcium
pantothenic
   

 Table (2) indicates the main application industries and materials:Thin Film Evaporator can be used for materials concentration, degassing, De-solvent (solvent recovery), purification etc. chemical unit operation. The following process can be considered as reference.
    ¢ÙMaterials concentration ( water evaporation) see figure (7)
    ¢ÚDe-solvent or purification figure (8)
    ¢ÛAs re-boiler of distillation tower (9)
    ¢ÜCombined with the tube type evaporator to form multiple effect evaporators see figure(10).
    6. The Thin Film Evaporator Selection
    The Thin Film Evaporator Selection need to consider multiple aspects elements and these elements also connect each other. General speaking, the following points need to be considered:
    ¢ÙThe evaporation Surface Determination:
    ¡øEvaporation volume calculation: According to the treated volume and in & out materials concentration to calculate evaporation volume per unit time.
    ¡øEstimate the evaporation strength based on the materials viscosity, concentration, evaporation temperature etc.
    ¡øConsider certain amount of access volume to calculate evaporation surface.
    ¢Ú Volume degree determination
    ¡øTo obtain vacuum degree will sacrifice energy consumptions, as long as meet the evaporation requirement, unnecessary to demand over high vacuum degree.
    ¡øVacuum degree under this evaporation temperature can be calculated according to materials heat sensitivity.
    ¡øConsider certain possible leakage and the resistance in second steam stream path to determine necessary vacuum degree.     ¢ÛScrapper type and materials determination
    ¡øTo select proper scrapper type is based on the materials viscosity, crystallization tendency, foam etc. physical and chemical characteristics, meanwhile consider evaporation temperature to determine proper materials.
    ¢ÜHeating Media Determination
    ¡øAccording to required evaporation temperature and heat energy consumption, the proper heating media will be decided, possible use steam, or hot water and heating oil etc.
    ¢ÝEvaporator Materials Selection
    ¢ÞMotor Explosion Proof Property Selection and Determination
    According to our company many years practice experiences, motors with proper type and specification will be selected to help customer use.

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Evaporation disillation Contact:13255219688 lai jing liang