1. Introduction
GXZ Series Rotation Thin Film Evaporator
manufactured by Wuxi Lima Chemical Machinery
Co.,Ltd. ( former Wuxi Chemical Machinery Factory
) is a new type of high efficiency evaporator
which uses rotating scratch blade to force forming
film and create falling film evaporation under
vacuum condition. It has big heat transferring
coefficient, high evaporation strength, short
overflow time, flexible operation property etc.
advantages, suitable for heat sensitive materials,
high viscose materials, and easy crystallization,
containing powder materials evaporation,
concentration, degassing, de-solving, distillation
purification. Due to these advantages, it is
widely used in petrochemical, chemical,
pharmaceutics, pesticide, daily chemical, food
processing and fine chemical industries.
We have manufactured this type equipment for more
than 10 years and gained plenty of fabrication and
application experiences. According to market
demanding, combined with customer¡¯s production
requirements, and to meet clients¡¯ process
requirement, we select optimized equipment
structure to assure reliable and top fabrication
quality. By improving fabrication equipment,
testing method and production design, we reached
remarkable achievements. We are at domestic
leading position in technical level and products
quality. This product has passed Jiangsu
Provincial Science and Technological Achievements
Appraisal ( No.03,1994) in Jan.,1994 and received
¡°National Grade New Product Honor¡± in 1995 and
applied Patent from China Patent Bureau in 1999 (
Patent No. ZL 99 2 28920.3).
2. Structure
GXZ Series Thin Film Evaporator Main Structure see
Figure 1, The detailed components see the
following description:
a. Motor, Speed Reducer
It is the device driven by rotor rotation. The
rotor rotation speed is decided by scraper shape,
materials viscosity and the inner diameter of
evaporation column. To select proper scraper
linear velocity is one of the important parameters
to assure evaporator stable and reliable operation
and get satisfaction of evaporation result.
b. Separation Column
The materials enter the evaporator in the inlet
located at the bottom of separation column by
tangent direction and uniformly distributed on the
inner wall of evaporator column by distributor in
the column. The second time vapor evaporated from
evaporator column goes up to separation column,
the liquid drops and bubbles which possibly
entrained in the vapor will be separated out by
gas/liquid separator, the second time vapor goes
out from evaporator through top location exit.
The optimized design of separation column based on
the evaporator inner resistance calculation is the
key element of avoiding materials ¡°short cut¡±.
(¡°Short Cut¡± means that the entered materials
fail to complete evaporation process but escape
from the second time vapor exit of evaporator).
c. Distributor
The distributor is located on the rotor. The
rational design makes materials enter evaporator
in tangent direction ( see figure 1 indication )
and continuously , uniformly to be distributed on
evaporation surface in film form.
d. Gas/Liquid Separator
The rotating scraper type gas/liquid separator is installed on the up location of the separation column. The function is to capture entrained liquid drops and bubbles in the second time vapor and make them to drop back to the evaporation surface.
e. Evaporation Column
Also called Heating Column. It is the heat exchanging evaporation surface between materials film, which is formed to be forced by rotating scraper and heating medium in the jacket. The inner diameter and length of heating column are determined by evaporation surface and proper length/diameter ratio.
The heating column inner wall is machined and polished by special machinery and formed with both ends flange connection surface in one time, which assures the whole equipment roundness. After polishing ( if necessary mirror polishing), the inner wall of the column is smooth and brilliant, not easy to stick materials and scared, as a result, effectively assures equipment high heat transfer coefficient.
¢ÙThe jacket
is used for column heating if the heating
media is steam.
¢ÚThe half pipe
shape jacket is used for column heating,
if the heating media is heat oil or high
pressure steam.
f. Rotor
The rotor
installed in evaporator inside consists of
rotating shaft and support. The rotor
driven by motor and speed reducer brings
scraper to make circular movement. The
support is made stainless steel and
machined in precise dimensions to assure
the strength, dimension, and stability
etc. properties.
g. Scraper
The scraper
movement makes materials form thin film
continuously on evaporator surface to
reach the thin film evaporation results.
According to
viscosity of the materials, the following
three types scrapers can be selected:
¢ÙSlide Scraper
(see figure 2)
Sliding scraper is a
basic and normal scraper. The scrapers are
installed in the four guiding grooves on the
rotor. Due to the rotation centrifugal
force, the scrapers circular movement force
materials to move towards column inner wall
in radial direction and make the materials
on evaporation surface in film turbulent
form. Thus, greatly increase the heat
transfer coefficient and effectively avoid
materials overheat, drying wall and scarring
etc. problems.
The scrapers use PTFE as packing materials, it is suitable at 150¡æ working temperature. If the evaporation temperature is above 150¡æ,carbon fiber materials will be used as packing. The scraper end surface is machined to form certain angular liquid guide groove.
¢ÚFixed
Scraper see (figure 3) Fixed
in rotor, the scraper is made of metal
materials, The gap distance between rotating
scraper and the inner wall of column is only
1-2mm. It requires high fabrication and
installation precision. It is suitable for
high viscose and easy bubbling materials
evaporation and concentration, de-solving
and extraction. ¢ÛHinge
Scraper ( See Figure 4)
e. Short
flow pass
The flow time in the
evaporator is very short. Less than 10
seconds. For normal use scraper, there is
flow-guiding groove on the scraper end face,
usually the slope angle is 45. To change the
slope angle may change materials flow time.
The material scrapped by scraper leaves
evaporator sector in screw falling status.
To shorter flow time will effectively
prevent from products decomposing,
polymerization and deterioration.
f. Low quality steam
can be used.
Steam is commonly
used heating media. Because the materials
boiling point is decreased, as long as
assuring the same ¦¤t condition, the heating
media temperature can be decreased. To use
low quality vapor is helpful for energy
multiple use, especially suitable for the
end evaporator of multiple-effect
evaporation.
g. Versatile
Suitability, Easy Operation
Unique structure
design makes this equipment possibly treat
high viscosity, particle containing, heat
sensitive and easy crystallization materials
which the normal evaporator is difficult to
treat with.
The rotation thin
film evaporator has wide operation range,
stable working status, and easy maintenance.
4. Products
Specification
Specification
Definition for GXZ High Efficiency Rotation
Thin Film Evaporator:
GXZ High Efficiency
Rotation Thin Film Evaporator Dimensions and
partly Technical Parameters see Figure 6 and
Table 1
Figure 1: GXZ High
Efficiency Rotation Thin Film Evaporator
Dimensions and partly Technical Parameters
see Figure 6 and Table 1
Evaporation
Surface
(m2)
Size
Equip.
Total
Height
A
Heating
Column
Height
B
Feeding
Materials
Separation
Column
C
Column
OD.
D
Support
Height
E
Motor
Speed
Reducer
F
Hole
Gap
of
Support
G
Dn
0.3
2290
750
550
273
1253
702
480
211
0.5
2440
900
550
273
1403
702
480
211
1
2820
1200
550
412
1781
702
605
313
2
4330
1830
755
462
2372
1433
843
400
4
5490
2630
844
712
3511
1565
1003
600
6
6275
2890
844
912
3817
1944
1236
800
8
6910
3658
844
916
4587
1909
1236
800
10
6960
3658
900
1112
4542
1918
1236
1000
12
7460
3658
1003
1316
4985
1998
1567
1200
15
8315
4590
1003
1316
4390
2040
1804
1200
18
9210
5494
1003
1316
5290
2040
1804
1200
20
9840
6121
1003
1316
5920
2040
1804
1200
Evaporation
Surface
(m2)
Equipment
Motor Power
(kW)
Pressure (Mpa)
Total weight
(about)(Kg)
Jacket
Inner Column
0.3
1.5
0.6
£¼-0.095
480
0.5
1.5
0.6
£¼-0.095
500
1
1.5
0.6
£¼-0.095
680
2
3.0
0.4
£¼-0.095
1100
4
5.5
0.4
£¼-0.095
1950
6
7.5
0.4
£¼-0.095
2980
8
7.5
0.4
£¼-0.095
3550
10
7.5
0.4
£¼-0.095
4880
12
11
0.4
£¼-0.095
6300
15
15
0.4
£¼-0.095
7850
18
15
0.4
£¼-0.095
8830
20
15
0.4
£¼-0.095
9350
¢ÙThere are
possible change for the above dimensions in
actual equipment, reference only. Take the
drawings dimension as actual size after
signed purchase order.
¢ÚD indicates
jacket outer diameter; Dn indicates inner
diameter of evaporation column in the table.
¢ÛJacket Pressure:
Normally designed based on 0.4Mpa steam,
also can be designed per customer
requirement.
If heating oil is used, it can be designed
per the requirement.
¢ÜThe vacuum degree
in the inner evaporation column : Normally
designed based on -0.09Mpa(-680mmHg), also
can meet clients¡¯ requirement to reach
-0.095Mpa(about -720mmHg)and
-0.0986Mpa(about-750mmHg)£»
¢ÝMain Column (
Materials contacting parts) and jacket
materials: Per clients¡¯ actual
requirements, use SUS304¡¢316L¡¢316Ti¡¢.310Sor
Ti and Ni. Materials£»
¢ÞEquipment Total
Weight does not include materials weight.
5. Application
Industries and Operation Unit Sample
High Efficiency
Rotation Thin Film Evaporator has been
widely used for Chinese and West Medicine,
Agriculture Pesticide, Light Industry, Daily
Chemical, Biological Chemical, Fine
Chemical, Petrochemical etc. industries.
Excellent results have been received. See
Table (2), reference only.
Industry
Typical
Materials
Industry
Typical
Materials
Industry
Typical
Materials
Pharmaceu-
tics
Vitamin VE¡¢V
Inorganic
TiCl3
Organic
High
Concentration
Aldehyde
Chinese Herb
MnO2
Fine
terephthalic
salts
Anti-bacteria
Agent
Caustic Soda
Trihydroxymethyl
propane
Pharmaceutics
Solution
K2SO4
xanthate
aldehyde
Medical
Intermediate
KBr, NaBr
Poly ether
polyol
Nitrile Amine
Aluminum Sulfates
Peach glue
Azoles
Sodium Silicate
Polyacrylamine
Light
Industry
and
Daily
Chemical
Natural
Colorant
KNO3
Tetra-amino-
aniline
Lactic Acid
L-Lactic Acid
Potassium
permanganate
Tri-methyl
Quinone
Lacithin
Calcium sulfide
Epoxy Resin
Essence
Tungstic acid
Molybdic acid
Bis-phenol -A
Bee Honey
Sodium
Hydrosulfite
Rongalite
Methy,
Ethyl Ester
Carbonates
Glyceryl
Pesticide
Furan phenol
Hydroxyl
acetic acid
Animal Feed
Additives
Pyrethrin
Environment
Protection
Waste Water of
Sodium Sulfates
Starch
Glycogen
Ethyl ammonium
oxalate
Waste Water of
NaCl
Enzyme
Methamidophos
Waste Water of
NH4Cl
Alkyl
glyciside
Tetrahydrofuran
Waste Water of
(NH4)2SO4
Alcohol Ether
Sulfates
Weed-killer
Potassium
sorbate
Dextran
calcium
pantothenic
Table (2)
indicates the main application industries
and materials:Thin Film Evaporator can be
used for materials concentration, degassing,
De-solvent (solvent recovery), purification
etc. chemical unit operation. The following
process can be considered as reference.
¢ÙMaterials
concentration ( water evaporation) see
figure (7)
¢ÚDe-solvent or
purification figure (8)
¢ÛAs re-boiler of
distillation tower (9)
¢ÜCombined with the
tube type evaporator to form multiple effect
evaporators see figure(10).
6. The Thin Film
Evaporator Selection
The Thin Film
Evaporator Selection need to consider
multiple aspects elements and these elements
also connect each other. General speaking,
the following points need to be considered:
¢ÙThe evaporation
Surface Determination:
¡øEvaporation
volume calculation: According to the treated
volume and in & out materials
concentration to calculate evaporation
volume per unit time.
¡øEstimate the
evaporation strength based on the materials
viscosity, concentration, evaporation
temperature etc.
¡øConsider certain
amount of access volume to calculate
evaporation surface.
¢Ú Volume degree
determination
¡øTo obtain vacuum
degree will sacrifice energy consumptions,
as long as meet the evaporation requirement,
unnecessary to demand over high vacuum
degree.
¡øVacuum degree
under this evaporation temperature can be
calculated according to materials heat
sensitivity.
¡øConsider certain
possible leakage and the resistance in
second steam stream path to determine
necessary vacuum degree.
¢ÛScrapper type and
materials determination
¡øTo select proper
scrapper type is based on the materials
viscosity, crystallization tendency, foam
etc. physical and chemical characteristics,
meanwhile consider evaporation temperature
to determine proper materials.
¢ÜHeating Media
Determination
¡øAccording to
required evaporation temperature and heat
energy consumption, the proper heating media
will be decided, possible use steam, or hot
water and heating oil etc.
¢ÝEvaporator
Materials Selection
¢ÞMotor Explosion
Proof Property Selection and Determination
According to our
company many years practice experiences,
motors with proper type and specification
will be selected to help customer use.